Hanna-instruments HI 83211 Manual do Utilizador

Consulte online ou descarregue Manual do Utilizador para Instrumentos de medida Hanna-instruments HI 83211. Hanna Instruments HI 83211 User Manual Manual do Utilizador

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Página 1 - HI 83211

1Instruction ManualHI 83211Multiparameter BenchPhotometerfor Chemical Manufacturerswww.hannainst.com

Página 2 - TABLE OF CONTENTS

10• Pay attention to push the cuvette completely down in the holder and to align the white point on thecap to the indexing mark on the meter.• In orde

Página 3 - PRELIMINARY EXAMINATION

11• The chemicals contained in the reagent kits may be hazardous if improperly handled.• Read the Material Safety Data Sheet (MSDS) before performing

Página 4 - PRINCIPLE OF OPERATION

12POWER CONNECTION AND BATTERY MANAGEMENTThe meter can be powered from an AC/DC adapter (included) or from the built-in rechargeable battery.Note: Alw

Página 5

13DATA MANAGEMENTThe instrument features a data log function to help you keep track of all your analysis. The data log canhold 200 individual measurem

Página 6 - FUNCTIONAL DESCRIPTION

14In the Setup mode the instrument’s parameters can be changed. Some parameters affect the measuringsequence and others are general parameters that ch

Página 7 - KEYPAD DESCRIPTION

15Date / TimeThis option is used to set the instrument’s date and time.Press the Modify key to change the date/time.Press the W X functional keys to h

Página 8

16HI 83211 offers an interactive contextual help mode that assists the user at any time.To access the help screens press HELP.The instrument will disp

Página 9 - USING CUVETTES

17AluminumSPECIFICATIONSRange 0.00 to 1.00 mg/LResolution 0.01 mg/LAccuracy ±0.02 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight Sou

Página 10 - INTERFERENCES

18• Add the content of one packet of HI 93712C-0 Bleachingpowder to one of the two cuvettes. Replace the cap and shakevigorously until completely diss

Página 11 - HEALTH & SAFETY

1910 mLAmmonia MRSPECIFICATIONSRange 0.00 to 10.00 mg/LResolution 0.01 mg/LAccuracy ±0.05 mg/L ±5% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationL

Página 12 - OPERATIONAL GUIDE

2Dear Customer,Thank you for choosing a Hanna product. Please read this instruction manual carefully before using theinstrument. This manual will prov

Página 13 - CHEMICAL FORM

20• Remove the cuvette.• Add 4 drops of HI 93715A-0 First Reagent (6 drops forseawater analysis). Replace the cap and mix the solution.• Add 4 drops o

Página 14 - SETUPSETUP

2110 mLAmmonia LRSPECIFICATIONSRange 0.00 to 3.00 mg/LResolution 0.01 mg/LAccuracy ±0.04 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLi

Página 15

22Ammonia LR• Remove the cuvette.• Add 4 drops of HI 93700A-0 First Reagent (6 drops forseawater analysis). Replace the cap and mix the solution.• Add

Página 16 - HELP MODEHELP MODE

23Chromium VI HRSPECIFICATIONSRange 0 to 1000 μg/LResolution 1 μg/LAccuracy ±5 μg/L ±4% of reading at 25 °CTypical EMC ±1 μg/LDeviationLight Source Tu

Página 17 - ALUMINUM

24• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitfor

Página 18

25Chromium VI LRSPECIFICATIONSRange 0 to 300 μg/LResolution 1 μg/LAccuracy ±1 μg/L ±4% of reading at 25 °CTypical EMC ±1 μg/LDeviationLight Source Tun

Página 19 - AMMONIA MEDIUM RANGE

26• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitfor

Página 20

27Copper HRSPECIFICATIONSRange 0.00 to 5.00 mg/LResolution 0.01 mg/LAccuracy ±0.02 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight So

Página 21 - AMMONIA LOW RANGE

28Copper HR• Remove the cuvette.• Add the content of one packet of HI 93702-0 Bicinchoninate.Replace the cap and shake gently for about 15 seconds.• R

Página 22

29Copper LRSPECIFICATIONSRange 0 to 1000 μg/LResolution 1 μg/LAccuracy ±10 μg/L ±5% of reading at 25 °CTypical EMC ±1 μg/LDeviationLight Source Tungst

Página 23 - CHROMIUM VI HIGH RANGE

3EPA: US Environmental Protection Agency°C: degree Celsius°F: degree Fahrenheitμg/L: micrograms per liter (ppb)mg/L: milligrams per liter (ppm)g/L: gr

Página 24

30Copper LR• Remove the cuvette.• Add the content of one packet of HI 95747-0 Bicinchoninate.Replace the cap and shake gently for about 15 seconds.• R

Página 25 - CHROMIUM VI LOW RANGE

31Cyanuric AcidSPECIFICATIONSRange 0 to 80 mg/LResolution 1 mg/LAccuracy ±1 mg/L ±15% of reading at 25 °CTypical EMC ±1 mg/LDeviationLight Source Tung

Página 26

32Cyanuric Acid• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternati

Página 27 - COPPER HIGH RANGE

33SPECIFICATIONSRange 0.0 to 12.5 mg/LResolution 0.1 mg/LAccuracy ±0.1 mg/L ±5% of reading at 25 °CTypical EMC ±0.1 mg/LDeviationLight Source Tungsten

Página 28

34Iodine• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternatively, w

Página 29 - COPPER LOW RANGE

35Iron HRSPECIFICATIONSRange 0.00 to 5.00 mg/LResolution 0.01 mg/LAccuracy ±0.04 mg/L ±2% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight Sour

Página 30

36Iron HR• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternatively,w

Página 31 - CYANURIC ACID

37Iron LRSPECIFICATIONSRange 0 to 400 μg/LResolution 1 μg/LAccuracy ±10 μg/L ±8% of reading at 25 °CTypical EMC ±1 μg/LDeviationLight Source Tungsten

Página 32 - Cyanuric Acid

38Iron LR• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready formeasurement.• Remove the cuvette.• Fill another gra

Página 33 - MEASUREMENT PROCEDURE

39Iron LRINTERFERENCESInterference may be caused by:Cadmium above 4.0 mg/LChromium3+ above 0.25 mg/LChromium6+ above 1.2 mg/LCobalt above 0.05 mg/LCop

Página 34

4PRECISION AND ACCURACYPrecision is how closely repeated measurements agreewith each other. Precision is usually expressed asstandard deviation (SD).A

Página 35 - IRON HIGH RANGE

40MolybdenumSPECIFICATIONSRange 0.0 to 40.0 mg/LResolution 0.1 mg/LAccuracy ±0.3 mg/L ±5% of reading at 25 °CTypical EMC ±0.1 mg/LDeviationLight Sourc

Página 36

41• Fill one graduated mixing cylinder up to the 25 mLmark with the sample.• Add the content of one packet of HI 93730A-0molybdenum reagent, close the

Página 37 - IRON LOW RANGE

42Molybdenum• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitfor five minutes and press Read. Whe

Página 38

43Nickel HRSPECIFICATIONSRange 0.00 to 7.00 g/LResolution 0.01 g/LAccuracy ±0.07 ±4% of reading at 25 °CTypical EMC ±0.02 g/LDeviationLight Source Tun

Página 39

44Nickel HR• Remove the cuvette and add the content of one packet ofHI 93726-0 reagent. Replace the cap and shake gentlyuntil completely dissolved.• R

Página 40 - MOLYBDENUM

45 Nickel LRSPECIFICATIONSRange 0.000 to 1.000 mg/LResolution 0.001 mg/LAccuracy ±0.010 mg/L ±7% of reading at 25 °CTypical EMC ±0.001 mg/LDeviationLi

Página 41 - Molybdenum

46Nickel LR• Press Timer and the display will show a countdown prior to adding reagent C or, alternatively, waitfor 15 minutes. Add one packet of HI 9

Página 42

47INTERFERENCESInterference may be caused by:Co2+ must not be presentFe2+ must not be presentAl3+ above 32 mg/LCa2+ above 1000 mg/L (as CaCO3)Cd2+ abo

Página 43 - NICKEL HIGH RANGE

48pHSPECIFICATIONSRange 6.5 to 8.5 pHResolution 0.1 pHAccuracy ±0.1 pH at 25 °CTypical EMC ±0.1 pHDeviationLight Source Tungsten lamp with narrow band

Página 44

49pH• Remove the cuvette and add 5 drops of HI 93710-0 PhenolRed Indicator. Replace the cap and mix the solution.• Reinsert the cuvette into the instr

Página 45 - NICKEL LOW RANGE

5Where:-log I/Io= Absorbance (A)Io= intensity of incident light beamI = intensity of light beam after absorptionελ= molar extinction coefficient at wa

Página 46 - Nickel LR

50Phosphate HRSPECIFICATIONSRange 0.0 to 30.0 mg/LResolution 0.1 mg/LAccuracy ±1 mg/L ±4% of reading at 25 °CTypical EMC Dev. ±0.1 mg/LLight Source Tu

Página 47

51Phosphate HR• Add the content of one packet of HI 93717B-0 PhosphateHR Reagent B to the cuvette. Replace the cap and shakegently until completely di

Página 48

52Phosphate LRSPECIFICATIONSRange 0.00 to 2.50 mg/LResolution 0.01 mg/LAccuracy ±0.04 mg/L ±4% of reading at 25 °CTypical EMC Dev. ±0.01 mg/LLight Sou

Página 49

53Phosphate LR• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternativ

Página 50 - PHOSPHATE HIGH RANGE

54PhosphorusSPECIFICATIONSRange 0.0 to 15.0 mg/LResolution 0.1 mg/LAccuracy ±0.3 mg/L ±4% of reading at 25 °CTypical EMC Dev. ±0.2 mg/LLight Source Tu

Página 51

55Phosphorus• Add the content of one packet of HI 93706B-0 PhosphorusReagent B (Amino Acid) to the cuvette. Replace the capand shake gently until comp

Página 52 - PHOSPHATE LOW RANGE

56SilicaSPECIFICATIONSRange 0.00 to 2.00 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight Sourc

Página 53

57Silica• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready for measurement.• Remove the cuvette and add the conten

Página 54 - PHOSPHORUS

58SilverSPECIFICATIONSRange 0.000 to 1.000 mg/LResolution 0.005 mg/LAccuracy ±0.020 mg/L ±5% of reading at 25 °CTypical EMC ± 0.001 mg/LDeviationLight

Página 55

59Silver• Add exactly 1.0 mL of HI 93737B-0 Buffer reagent to the secondbeaker (the sample) and swirl gently to mix. Press Timer and thedisplay will s

Página 56

61) Open Cuvette Lid2) Indexing mark3) Cuvette point4) Liquid Crystal Display (LCD)5) Splash proof keypad6) ON/OFF power switch7) Power input connecto

Página 57

60Silver• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready formeasurement.• Fill a second cuvette up to the mark w

Página 58

61ZincSPECIFICATIONSRange 0.00 to 3.00 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight Source

Página 59

62INTERFERENCESInterference may be caused by:Aluminum above 6 mg/LCadmium above 0.5 mg/LCopper above 5 mg/LIron above 7 mg/LManganese above 5 mg/LNick

Página 60

63The instrument shows clear warning messages when erroneous conditions appear and when measured values areoutside the expected range. These messages

Página 61 - REQUIRED REAGENT

64The analyzed data can be managed using Hanna’s product HI92000, Windows® Compatible Software.Windows® is registered Trademark of "Microsoft Co.

Página 62

65Description Range MethodAmmonia MR 0.00 to 10.00 mg/L NesslerAmmonia LR 0.00 to 3.00 mg/L NesslerChromium VI HR 0 to 1000 μg/L Diphenylcarbohydrazid

Página 63 - ERRORS AND WARNINGS

66OTHER ACCESSORIESHI 731318 cloth for wiping cuvettes (4 pcs)HI 731321 glass cuvettes (4 pcs)HI 731325W new cap for cuvette (4 pcs)HI 740034 cap for

Página 64

67All Hanna Instruments meters are warranted for two years against defects in workmanship and materialswhen used for its intended purpose and maintain

Página 65 - STANDARD METHODS

68Printed in EUROPE(ROMANIA)Hanna Instruments Inc.Highland Industrial Park584 Park East DriveWoonsocket, RI 02895 USATechnical Support for CustomersTe

Página 66 - ACCESSORIES

7KEYPAD DESCRIPTIONThe keypad contains 8 direct keys and 3 functional keys with the following functions:Press to perform the function displayed above

Página 67 - WARRANTY

8The instructions listed below should be carefully followed during testing to ensure most accurate results.• Color or suspended matter in large amount

Página 68 - MAN83211 04/10

9• Proper use of the powder reagent packet:(a) use scissors to open the powder packet;(b) push the edges of the packet to form a spout;(c) pour out th

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