Hanna-instruments HI 83099 Manual do Utilizador

1Instruction ManualHI 83099COD and Multiparameter BenchPhotometerwww.hannainst.com

1918• Remove the cap and fill the Demineralizer Bottle with tap water.• Replace the cap and shake gently for at least 2 minutes.• Open the upper part

2120AluminumALUMINUMSPECIFICATIONSRange 0.00 to 1.00 mg/LResolution 0.01 mg/LAccuracy ±0.02 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/LDeviatio

232210 mLSPECIFICATIONSRange 0 to 500 mg/L (as CaCO3)Resolution 5 mg/LAccuracy ±5 mg/L ±10 % of reading at 25 °CTypical EMC ±5 mg/LDeviationLight Sour

252410 mLAmmonia MRSPECIFICATIONSRange 0.00 to 10.00 mg/LResolution 0.01 mg/LAccuracy ±0.05 mg/L ±5% of reading at 25 °CTypical EMC ±0.01 mg/LDeviatio

272610 mLAmmonia LRSPECIFICATIONSRange 0.00 to 3.00 mg/LResolution 0.01 mg/LAccuracy ±0.04 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/LDeviation

2928BromineBROMINESPECIFICATIONSRange 0.00 to 8.00 mg/LResolution 0.01 mg/LAccuracy ±0.08 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationL

3130CALCIUMSPECIFICATIONSRange 0 to 400 mg/LResolution 10 mg/LAccuracy ±10 mg/L ±5% of reading at 25 °CLight Source Tungsten lamp with narrow band int

3332FREE CHLORINEFREE CHLORINEFREE CHLORINEFREE CHLORINEFREE CHLORINESPECIFICATIONSRange 0.00 to 2.50 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3%

3534• Place the cuvette into the instrument.• Press Read to start the reading. The instrument displays the results in mg/L of free chlorine.INTERFEREN

3736Total Chlorine• Press the Zero key. The meter will show “-0.0-” when the meter is zeroed and ready for measurement.• Remove the cuvette.Powder rea

32PRELIMINARY EXAMINATIONPlease examine this product carefully. Make sure that the instrument is not damaged. If any damageoccurred during shipment, p

3938Chlorine DioxideCHLORINE DIOXIDESPECIFICATIONSRange 0.00 to 2.00 mg/LResolution 0.01 mg/LAccuracy ±0.10 mg/L ±5% of reading at 25 °CTypical EMC ±0

4140Chlorine Dioxide• Press the Zero key. The meter will show “-0.0-” when the meter is zeroed and ready formeasurement.• Fill another cuvette with 10

4342• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitf

4544• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitf

4746Color of Water# 3• Fill the second cuvette up to the mark with unfiltered sampleand replace the cap. This is the apparent color.• Filter 10 mL of

4948Copper HR• Remove the cuvette.• Add the content of one packet of HI 93702-0 Bicinchoninate.Replace the cap and shake gently for about 15 seconds.•

5150Copper LR• Remove the cuvette.• Add the content of one packet of HI 95747-0 Bicinchoninate.Replace the cap and shake gently for about 15 seconds.•

5352Cyanuric Acid• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alterna

5554• Press Timer and the display will show the countdown prior to zeroing the blank or, alternatively, waitfor two minutes and press Zero. The displa

5756Hardness Ca• Add 1 drop of HI 93720C-0 EGTA solution to one cuvette (# 1), replacethe cap and invert the cuvette several times to mix. This is the

54PRINCIPLE OF OPERATIONAbsorption of light is a typical phenomenon of interaction between electromagnetic radiation and matter.When a light beam cros

5958 Hardness MgMAGNESIUM HARDNESSSPECIFICATIONSRange 0.00 to 2.00 mg/LResolution 0.01 mg/LAccuracy ±0.11 mg/L ±5% of reading at 25 °CTypical EMC ±0.0

6160Hardness Mg• Press s or t to access the second level functions.• Press the Chem Frm key to convert the result in mg/L of Magnesium (Mg2+).• Press

6362• Add 12 drops of the HI 93704-0 reagent toeach cuvette. Replace the caps and shakegently to mix (about 30 seconds).• Place the blank (#1) into th

6564Iodine• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternatively,

6766Iron HR• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternatively

6968Iron LR• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready formeasurement.• Remove the cuvette.• Fill another g

7170MagnesiumSPECIFICATIONSRange 0 to 150 mg/LResolution 5 mg/LAccuracy ±5 mg/L ±3% of reading at 25 °CLight Source Tungsten lamp with narrow band int

7372SPECIFICATIONSRange 0.0 to 20.0 mg/LResolution 0.1 mg/LAccuracy ±0.2 mg/L ±3% of reading at 25 °CTypical EMC ±0.1 mg/LDeviationLight Source Tungst

7574Manganese LRMANGANESE LOW RANGESPECIFICATIONSRange 0 to 300 µg/LResolution 1 µg/LAccuracy ±10 µ/L ±3% of reading at 25 °CTypical EMC ±1 µg/LDeviat

7776Manganese LR• Insert the second cuvette with the reacted sample into the instrument.• Press Read to start the reading. The instrument displays the

76KEYPAD DESCRIPTIONThe keypad contains 8 direct keys and 3 functional keys with the following functions:Press to perform the function displayed above

7978• Fill one graduated mixing cylinder up to the 25 mLmark with the sample.• Add the content of one packet of HI 93730A-0molybdenum reagent, close t

8180Nickel HRSPECIFICATIONSRange 0.00 to 7.00 g/LResolution 0.01 g/LAccuracy ±0.07 ±4% of reading at 25 °CTypical EMC ±0.02 g/LDeviationLight Source T

8382 Nickel LRNICKEL LOW RANGESPECIFICATIONSRange 0.000 to 1.000 mg/LResolution 0.001 mg/LAccuracy ±0.010 mg/L ±7% of reading at 25 °CTypical EMC ±0.0

8584INTERFERENCESInterference may be caused by:Co2+ must not be presentFe2+ must not be presentAl3+ above 32 mg/LCa2+ above 1000 mg/L (as CaCO3)Cd2+ a

8786 Nitrate• Replace the cap and immediately shake vigorously upand down for exactly 10 seconds. Continue to mix byinverting the cuvette gently for 5

8988Nitrite HR• Add the content of one packet of HI 93708-0 reagent.Replace the cap and shake gently until completelydissolved.• Reinsert the cuvette

9190• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitf

9392Dissolved Oxygen• Let the sample stand and the flocculent agent will start to settle.• After approximately 2 minutes, when the upper half of the b

9594SampleBlankBlankD.I. WaterSampleSample• Choose a homogeneous sample. Samples containing settleable solids need to be homogenized with ablender.• P

9796OXYGEN DEMAND, CHEMICAL MEDIUM RANGESPECIFICATIONSRange 0 to 1500 mg/L CODResolution 1 mg/LAccuracy ±15 mg/L or ±4 % of reading @ 25 °C, whichever

98• Proper use of the powder reagent packet:(a) use scissors to open the powder packet;(b) push the edges of the packet to form a spout;(c) pour out t

9998BlankSampleBlankSampleBlankD.I. WaterSampleSampleCOD MR• Select the Oxygen Demand, ChemicalMR (COD) method following one of theprocedures describe

101100BlankSampleBlankD.I. WaterSampleSampleSampleBlank• Choose a homogeneous sample. Samples containing settleable solids need to be homogenized with

103102OZONESPECIFICATIONSRange 0.00 to 2.00 mg/LResolution 0.01 mg/LAccuracy ±0.02 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight So

105104• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready formeasurement.• Remove the cuvette.• Add the content of

107106pH• Remove the cuvette and add 5 drops of HI 93710-0 PhenolRed Indicator. Replace the cap and mix the solution.• Reinsert the cuvette into the i

109108Phosphate HR• Add the content of one packet of HI 93717B-0 PhosphateHR Reagent B to the cuvette. Replace the cap and shakegently until completel

111110Phosphate LR• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, altern

113112Phosphorus• Add the content of one packet of HI 93706B-0 PhosphorusReagent B (Amino Acid) to the cuvette. Replace the capand shake gently until

115114• Remove the cuvette and add the content of one packet ofHI 93750B-0 reagent. Replace the cap and gently mix forone minute by slowly turning the

117116• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready for measurement.• Remove the cuvette and add the content

1110METHOD REFERENCE TABLEHEALTH & SAFETY• The chemicals contained in the reagent kits may be hazardous if improperly handled.• Read the Material

119118• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready for measurement.• Remove the cuvette and add the content

121120Silica• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready for measurement.• Remove the cuvette and add the co

123122Silver• Add exactly 1.0 mL of HI 93737B-0 Buffer reagent to the secondbeaker (the sample) and swirl gently to mix. Press Timer and thedisplay wi

125124SPECIFICATIONSRange 0 to 100 mg/LResolution 5 mg/LAccuracy ±5 mg/L ±3% of reading at 25 °CLight Source Tungsten lamp with narrow band interferen

127126ZincZINCSPECIFICATIONSRange 0.00 to 3.00 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight

129128The instrument shows clear warning messages when erroneous conditions appear and when measured values areoutside the expected range. These messa

131130Description Range MethodAluminum 0.00 to 1.00 mg/L AluminonAlkalinity 0 to 500 mg/L ColorimetricAmmonia MR 0.00 to 10.00 mg/L NesslerAmmonia LR

133132HI 93717-01 100 phosphate HR testsHI 93717-03 300 phosphate HR testsHI 93718-01 100 iodine testsHI 93718-03 300 iodine testsHI 93719-01 100 Mg h

135134WARRANTYAll Hanna Instruments meters are warranted for two years against defects in workmanship and materialswhen used for its intended purpose

136Printed in EUROPE(ROMANIA)Hanna Instruments Inc.Highland Industrial Park584 Park East DriveWoonsocket, RI 02895 USATechnical Support for CustomersT

1312DATA MANAGEMENTThe instrument features a data log function to help you keep track of all your analysis. The data log canhold 200 individual measur

1514Date / TimeThis option is used to set the instrument’s date and time.Press the Modify key to change the date/time.Press the ⊳ u functional keys to

1716SAMPLE PREPARATIONSAMPLE PREPARATION PROCEDUREThe following Sample Preparation Procedure applies in case of:• Samples with color or suspended matt