Hanna-instruments HI 83210-01 Manual do Utilizador

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Página 1 - HI 83210

1Instruction ManualHI 83210Multiparameter BenchPhotometerfor Pulp & Paper Millswww.hannainst.com

Página 2 - TABLE OF CONTENTS

10• Pay attention to push the cuvette completely down in the holder and to align the white point on thecap to the indexing mark on the meter.• In orde

Página 3 - GENERAL DESCRIPTION

11METHOD REFERENCE TABLEMethod Method Pagedescription1 Aluminum 172 Free Chlorine 193 Total Chlorine 224 Chlorine Dioxide 255 Color of Water 286 Disso

Página 4 - PRECISION AND ACCURACY

12POWER CONNECTION AND BATTERY MANAGEMENTThe meter can be powered from an AC/DC adapter (included) or from the built-in rechargeable battery.Note: Alw

Página 5

13DATA MANAGEMENTThe instrument features a data log function to help you keep track of all your analysis. The data log canhold 200 individual measurem

Página 6 - FUNCTIONAL DESCRIPTION

14In the Setup mode the instrument’s parameters can be changed. Some parameters affect the measuringsequence and others are general parameters that ch

Página 7 - KEYPAD DESCRIPTION

15Date / TimeThis option is used to set the instrument’s date and time.Press the Modify key to change the date/time.Press the W X functional keys to h

Página 8

16HI 83210 offers an interactive contextual help mode that assists the user at any time.To access the help screens press HELP.The instrument will disp

Página 9 - USING CUVETTES

17AluminumALUMINUMSPECIFICATIONSRange 0.00 to 1.00 mg/LResolution 0.01 mg/LAccuracy ±0.02 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationL

Página 10 - INTERFERENCES

18Aluminum• Add the content of one packet of HI 93712C-0 Bleachingpowder to one of the two cuvettes. Replace the cap and shakevigorously until complet

Página 11 - HEALTH & SAFETY

19Free ChlorineFREE CHLORINESPECIFICATIONSRange 0.00 to 2.50 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/L

Página 12 - OPERATIONAL GUIDE

2Dear Customer,Thank you for choosing a Hanna product. Please read this instruction manual carefully before using theinstrument. This manual will prov

Página 13 - CHEMICAL FORM

20Free Chlorine• Press the Zero key. The meter will show “-0.0-” when the meter is zeroed and ready for measurement.• Remove the cuvette.Powder reagen

Página 14 - SETUPSETUP

21Free Chlorine• Reinsert the cuvette into the instrument.• Press Read to start the reading. The instrument displays the results in mg/L of free chlo

Página 15

22Total ChlorineTOTAL CHLORINESPECIFICATIONSRange 0.00 to 3.50 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg

Página 16 - HELP MODEHELP MODE

23Total Chlorine• Press the Zero key. The meter will show “-0.0-” when the meter is zeroed and ready for measurement.• Remove the cuvette.Powder reage

Página 17 - ALUMINUM

24Total Chlorine• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitfor 2 minutes and 30 seconds and

Página 18

25Chlorine DioxideCHLORINE DIOXIDESPECIFICATIONSRange 0.00 to 2.00 mg/LResolution 0.01 mg/LAccuracy ±0.10 mg/L ±5% of reading at 25 °CTypical EMC ±0.0

Página 19 - FREE CHLORINE

26Chlorine Dioxide• Add the content of one packet of HI 93738B-0 Dechlorinating Reagent to one of the two cylinders(#1), close and invert it several t

Página 20 - Free Chlorine

27Chlorine Dioxide• Press the Zero key. The meter will show “-0.0-” when the meter is zeroed and ready formeasurement.• Fill another cuvette with 10 m

Página 21

28Color of WaterCOLOR OF WATERSPECIFICATIONSRange 0 to 500 PCU (Platinum Cobalt Units)Resolution 1 PCUAccuracy ±10 PCU ±5% of reading at 25 °CTypical

Página 22 - TOTAL CHLORINE

29Color of Water• Fill the second cuvette up to the mark with unfiltered sampleand replace the cap. This is the apparent color.• Filter 10 mL of sampl

Página 23 - Total Chlorine

3PRELIMINARY EXAMINATIONPlease examine this product carefully. Make sure that the instrument is not damaged. If any damageoccurred during shipment, pl

Página 24

30Dissolved OxygenDISSOLVED OXYGENSPECIFICATIONSRange 0.0 to 10.0 mg/LResolution 0.1 mg/LAccuracy ±0.4 mg/L ±3% of reading at 25 °CTypical EMC ± 0.1 m

Página 25 - CHLORINE DIOXIDE

31Dissolved Oxygen• Let the sample stand and the flocculent agent will start to settle.• After approximately 2 minutes, when the upper half of the bot

Página 26 - Chlorine Dioxide

32pHpHSPECIFICATIONSRange 6.5 to 8.5 pHResolution 0.1 pHAccuracy ±0.1 pH at 25 °CTypical EMC ±0.1 pHDeviationLight Source Tungsten lamp with narrow ba

Página 27 - SAMPLING PROCEDURE

33pH• Remove the cuvette and add 5 drops of HI 93710-0 PhenolRed Indicator. Replace the cap and mix the solution.• Reinsert the cuvette into the instr

Página 28 - COLOR OF WATER

34Phosphate HRPHOSPHATE HIGH RANGESPECIFICATIONSRange 0.0 to 30.0 mg/LResolution 0.1 mg/LAccuracy ±1 mg/L ±4% of reading at 25 °CTypical EMC Dev. ±0.1

Página 29 - Color of Water

35Phosphate HR• Add the content of one packet of HI 93717B-0 PhosphateHR Reagent B to the cuvette. Replace the cap and shakegently until completely di

Página 30 - DISSOLVED OXYGEN

36Phosphate LRPHOSPHATE LOW RANGESPECIFICATIONSRange 0.00 to 2.50 mg/LResolution 0.01 mg/LAccuracy ±0.04 mg/L ±4% of reading at 25 °CTypical EMC Dev.

Página 31

37Phosphate LR• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternativ

Página 32 - MEASUREMENT PROCEDURE

38SilicaSILICASPECIFICATIONSRange 0.00 to 2.00 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading reading at 25 °CTypical EMC ±0.01 mg/LDeviat

Página 33

39Silica• Place the cuvette into the holder and close the lid.• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready f

Página 34 - PHOSPHATE HIGH RANGE

4PRINCIPLE OF OPERATIONAbsorption of light is a typical phenomenon of interaction between electromagnetic radiation and matter.When a light beam cross

Página 35

40Silica• Press  or  to return to the measurement screen.INTERFERENCESInterference may be caused by:Phosphate above 60 mg/LPhosphate above 75 mg/LSu

Página 36 - PHOSPHATE LOW RANGE

41SilverSILVERSPECIFICATIONSRange 0.000 to 1.000 mg/LResolution 0.005 mg/LAccuracy ±0.020 mg/L ±5% of reading at 25 °CTypical EMC ± 0.001 mg/LDeviatio

Página 37

42Silver• Add exactly 1.0 mL of HI 93737B-0 Buffer reagent to the secondbeaker (the sample) and swirl gently to mix. Press Timer and thedisplay will s

Página 38

43Silver• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready formeasurement.• Fill a second cuvette up to the mark w

Página 39

44ZincZINCSPECIFICATIONSRange 0.00 to 3.00 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight Sou

Página 40

45ZincINTERFERENCESInterference may be caused by:Aluminum above 6 mg/LCadmium above 0.5 mg/LCopper above 5 mg/LIron above 7 mg/LManganese above 5 mg/L

Página 41

46The instrument shows clear warning messages when erroneous conditions appear and when measured values areoutside the expected range. These messages

Página 42

47The analyzed data can be managed using Hanna’s product HI92000, Windows® Compatible Software.DATA MANAGEMENTWindows® is registered Trademark of &quo

Página 43

48Description Range MethodAluminum 0.00 to 1.00 mg/L AluminonChlorine, Free 0.00 to 2.50 mg/L DPDChlorine, Total 0.00 to 3.50 mg/L DPDChlorine Dioxide

Página 44 - REQUIRED REAGENT

49OTHER ACCESSORIESHI 731318 cloth for wiping cuvettes (4 pcs)HI 731321 glass cuvettes (4 pcs)HI 731325W new cap for cuvette (4 pcs)HI 740034 cap for

Página 45

5Where:-log I/Io=Absorbance (A)Io=intensity of incident light beamI =intensity of light beam after absorptionελ=molar extinction coefficient at wavele

Página 46 - ERRORS AND WARNINGS

50WARRANTYAll Hanna Instruments meters are warranted for two years against defects in workmanship and materialswhen used for its intended purpose and

Página 47

51HANNA LITERATUREHanna publishes a wide range of catalogs and handbooks for an equally wide range of applications. Thereference literature currently

Página 48 - STANDARD METHODS

52Printed in EUROPE(ROMANIA)Hanna Instruments Inc.Highland Industrial Park584 Park East DriveWoonsocket, RI 02895 USATechnical Support for CustomersTe

Página 49 - ACCESSORIES

6INSTRUMENT DESCRIPTIONFUNCTIONAL DESCRIPTION1) Open Cuvette Lid2) Indexing mark3) Cuvette point4) Liquid Crystal Display (LCD)5) Splash proof keypad6

Página 50 - WARRANTY

7KEYPAD DESCRIPTIONThe keypad contains 8 direct keys and 3 functional keys with the following functions:Press to perform the function displayed above

Página 51 - HANNA LITERATURE

8The instructions listed below should be carefully followed during testing to ensure most accurate results.• Color or suspended matter in large amount

Página 52 - MAN83210 04/10

9• Proper use of the powder reagent packet:(a) use scissors to open the powder packet;(b) push the edges of the packet to form a spout;(c) pour out th

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