Hanna-instruments HI 83213-2008 Manual do Utilizador

1Instruction ManualHI 83213Multiparameter BenchPhotometerfor Municipal Wastewaterwww.hannainst.com

10• Pay attention to push the cuvette completely down in the holder and to align the white point on thecap to the indexing mark on the meter.• In orde

11METHOD REFERENCE TABLEMethod Method Pagedescription1 Aluminum 172 Ammonia MR 193 Ammonia LR 21 4 Bromine 235 Free Chlorine 256 Total Chlorine 2

12POWER CONNECTION AND BATTERY MANAGEMENTThe meter can be powered from an AC/DC adapter (included) or from the built-in rechargeable battery.Note: Alw

13DATA MANAGEMENTThe instrument features a data log function to help you keep track of all your analysis. The data log canhold 200 individual measurem

14SETUPSETUPSETUPSETUPSETUPIn the Setup mode the instrument’s parameters can be changed. Some parameters affect the measuringsequence and others are g

15Date / TimeThis option is used to set the instrument’s date and time.Press the Modify key to change the date/time.Press the W X functional keys to h

16HI 83213 offers an interactive contextual help mode that assists the user at any time.To access the help screens press HELP.The instrument will disp

17AluminumALUMINUMSPECIFICATIONSRange 0.00 to 1.00 mg/LResolution 0.01 mg/LAccuracy ±0.02 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationL

18Aluminum• Add the content of one packet of HI 93712C-0 Bleaching powder toone of the two cuvettes. Replace the cap and shake vigorously untilcomplet

19Ammonia MRAMMONIA MEDIUM RANGESPECIFICATIONSRange 0.00 to 10.00 mg/LResolution 0.01 mg/LAccuracy ±0.05 mg/L ±5% of reading at 25 °CTypical EMC ±0.01

2Dear Customer,Thank you for choosing a Hanna product. Please read this instruction manual carefully before using theinstrument. This manual will prov

20Ammonia MR• Remove the cuvette.• Add 4 drops of HI 93715A-0 First Reagent (6 drops forseawater analysis). Replace the cap and mix the solution.• Add

21Ammonia LRAMMONIA LOW RANGESPECIFICATIONSRange 0.00 to 3.00 mg/LResolution 0.01 mg/LAccuracy ±0.04 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/

22Ammonia LR• Remove the cuvette.• Add 4 drops of HI 93700A-0 First Reagent (6 drops forseawater analysis). Replace the cap and mix the solution.• Add

23BromineBROMINESPECIFICATIONSRange 0.00 to 8.00 mg/LResolution 0.01 mg/LAccuracy ±0.08 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLig

24Bromine• Remove the cuvette and add the content of one packet ofHI 93716-0 DPD reagent. Replace the cap and shake gently forabout 20 seconds to diss

25Free ChlorineFREE CHLORINESPECIFICATIONSRange 0.00 to 2.50 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/L

26Free Chlorine• Press the Zero key. The meter will show “-0.0-” when the meter is zeroed and ready for measurement.• Remove the cuvette.Powder reagen

27Free Chlorine• Reinsert the cuvette into the instrument.• Press Read to start the reading. The instrument displays the results in mg/L of free chlo

28Total ChlorineTOTAL CHLORINESPECIFICATIONSRange 0.00 to 3.50 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg

29Total Chlorine• Press the Zero key. The meter will show “-0.0-” when the meter is zeroed and ready for measurement.• Remove the cuvette.Powder reage

3PRELIMINARY EXAMINATIONPlease examine this product carefully. Make sure that the instrument is not damaged. If any damageoccurred during shipment, pl

30Total Chlorine• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitfor 2 minutes and 30 seconds and

31Chromium VI HRCHROMIUM VI HIGH RANGESPECIFICATIONSRange 0 to 1000 μg/LResolution 1 μg/LAccuracy ±5 μg/L ±4% of reading at 25 °CTypical EMC ±1 μg/LDe

32Chromium VI HR• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternat

33Chromium VI LRCHROMIUM VI LOW RANGESPECIFICATIONSRange 0 to 300 μg/LResolution 1 μg/LAccuracy ±1 μg/L ±4% of reading at 25 °CTypical EMC ±1 μg/LDevi

34Chromium VI LR• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternat

35Color of WaterCOLOR OF WATERSPECIFICATIONSRange 0 to 500 PCU (Platinum Cobalt Units)Resolution 1 PCUAccuracy ±10 PCU ±5% of reading at 25 °CTypical

36Color of Water• Fill the second cuvette up to the mark with unfiltered sampleand replace the cap. This is the apparent color.• Filter 10 mL of sampl

37Copper HRCOPPER HIGH RANGESPECIFICATIONSRange 0.00 to 5.00 mg/LResolution 0.01 mg/LAccuracy ±0.02 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/L

38Copper HR• Remove the cuvette.• Add the content of one packet of HI 93702-0 Bicinchoninate.Replace the cap and shake gently for about 15 seconds.• R

39Copper LRCOPPER LOW RANGESPECIFICATIONSRange 0 to 1000 μg/LResolution 1 μg/LAccuracy ±10 μg/L ±5% of reading at 25 °CTypical EMC ±1 μg/LDeviationLig

4PRINCIPLE OF OPERATIONAbsorption of light is a typical phenomenon of interaction between electromagnetic radiation and matter.When a light beam cross

40Copper LR• Remove the cuvette.• Add the content of one packet of HI 95747-0 Bicinchoninate.Replace the cap and shake gently for about 15 seconds.• R

41IODINEIodineSPECIFICATIONSRange 0.0 to 12.5 mg/LResolution 0.1 mg/LAccuracy ±0.1 mg/L ±5% of reading at 25 °CTypical EMC ±0.1 mg/LDeviationLight Sou

42Iodine• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternatively, w

43Nickel HRNICKEL HIGH RANGESPECIFICATIONSRange 0.00 to 7.00 g/LResolution 0.01 g/LAccuracy ±0.07 ±4% of reading at 25 °CTypical EMC ±0.02 g/LDeviatio

44Nickel HR• Remove the cuvette and add the content of one packet ofHI 93726-0 reagent. Replace the cap and shake gentlyuntil completely dissolved.• R

45 Nickel LRNICKEL LOW RANGESPECIFICATIONSRange 0.000 to 1.000 mg/LResolution 0.001 mg/LAccuracy ±0.010 mg/L ±7% of reading at 25 °CTypical EMC ±0.001

46Nickel LR• Press Timer and the display will show a countdown prior to adding reagent C or, alternatively, waitfor 15 minutes. Add one packet of HI 9

47Nickel LRINTERFERENCESInterference may be caused by:Co2+ must not be presentFe2+ must not be presentAl3+ above 32 mg/LCa2+ above 1000 mg/L (as CaCO3

48NitrateNITRATESPECIFICATIONSRange 0.0 to 30.0 mg/LResolution 0.1 mg/LAccuracy ±0.5 mg/L ±10% of reading at 25 °CTypical EMC ±0.1 mg/LDeviationLight

49Nitrate• Replace the cap and immediately shake vigorously upand down for exactly 10 seconds. Continue to mix byinverting the cuvette gently for 50 s

5Where:-log I/Io=Absorbance (A)Io=intensity of incident light beamI =intensity of light beam after absorptionελ=molar extinction coefficient at wavele

50Nitrite HRNITRITE HIGH RANGESPECIFICATIONSRange 0 to 150 mg/LResolution 1 mg/LAccuracy ±4 mg/L ±4% of reading at 25 °CTypical EMC ±1 mg/LDeviationLi

51Nitrite HR• Add the content of one packet of HI 93708-0 reagent.Replace the cap and shake gently until completely dissolved.• Reinsert the cuvette i

52Nitrite LRNITRITE LOW RANGESPECIFICATIONSRange 0.00 to 1.15 mg/LResolution 0.01 mg/LAccuracy ±0.06 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/

53Nitrite LR• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternativel

54Dissolved OxygenDISSOLVED OXYGENSPECIFICATIONSRange 0.0 to 10.0 mg/LResolution 0.1 mg/LAccuracy ±0.4 mg/L ±3% of reading at 25 °CTypical EMC ± 0.1 m

55Dissolved Oxygen• Let the sample stand and the flocculent agent will start to settle.• After approximately 2 minutes, when the upper half of the bot

56pHpHSPECIFICATIONSRange 6.5 to 8.5 pHResolution 0.1 pHAccuracy ±0.1 pH at 25 °CTypical EMC ±0.1 pHDeviationLight Source Tungsten lamp with narrow ba

57pH• Remove the cuvette and add 5 drops of HI 93710-0 PhenolRed Indicator. Replace the cap and mix the solution.• Reinsert the cuvette into the instr

58Phosphate HRPHOSPHATE HIGH RANGESPECIFICATIONSRange 0.0 to 30.0 mg/LResolution 0.1 mg/LAccuracy ±1 mg/L ±4% of reading at 25 °CTypical EMC Dev. ±0.1

59Phosphate HR• Add the content of one packet of HI 93717B-0 Phosphate HRReagent B to the cuvette. Replace the cap and shake gentlyuntil completely di

6INSTRUMENT DESCRIPTIONFUNCTIONAL DESCRIPTION1) Open Cuvette Lid2) Indexing mark3) Cuvette point4) Liquid Crystal Display (LCD)5) Splash proof keypad6

60Phosphate LRPHOSPHATE LOW RANGESPECIFICATIONSRange 0.00 to 2.50 mg/LResolution 0.01 mg/LAccuracy ±0.04 mg/L ±4% of reading at 25 °CTypical EMC Dev.

61Phosphate LR• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternativ

62PhosphorusPHOSPHORUSSPECIFICATIONSRange 0.0 to 15.0 mg/LResolution 0.1 mg/LAccuracy ±0.3 mg/L ±4% of reading at 25 °CTypical EMC Dev. ±0.2 mg/LLight

63Phosphorus• Add the content of one packet of HI 93706B-0 PhosphorusReagent B (Amino Acid) to the cuvette. Replace the capand shake gently until comp

64SilverSILVERSPECIFICATIONSRange 0.000 to 1.000 mg/LResolution 0.005 mg/LAccuracy ±0.020 mg/L ±5% of reading at 25 °CTypical EMC ± 0.001 mg/LDeviatio

65Silver• Add exactly 1.0 mL of HI 93737B-0 Buffer reagent to the secondbeaker (the sample) and swirl gently to mix. Press Timer and thedisplay will s

66Silver• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready formeasurement.• Fill a second cuvette up to the mark w

67ZincZINCSPECIFICATIONSRange 0.00 to 3.00 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight Sou

68ZincINTERFERENCESInterference may be caused by:Aluminum above 6 mg/LCadmium above 0.5 mg/LCopper above 5 mg/LIron above 7 mg/LManganese above 5 mg/L

69The instrument shows clear warning messages when erroneous conditions appear and when measured values areoutside the expected range. These messages

7KEYPAD DESCRIPTIONThe keypad contains 8 direct keys and 3 functional keys with the following functions:Press to perform the function displayed above

70The analyzed data can be managed using Hanna’s product HI92000, Windows® Compatible Software.DATA MANAGEMENTWindows® is registered Trademark of &quo

71Description Range MethodAluminum 0.00 to 1.00 mg/L AluminonAmmonia MR 0.00 to 10.00 mg/L NesslerAmmonia LR 0.00 to 3.00 mg/L NesslerBromine 0.00 to

72ACCESSORIESREAGENT SETSHI 93700-01 100 ammonia LR testsHI 93700-03 300 ammonia LR testsHI 93701-01 100 free chlorine tests (powder)HI 93701-03 300 f

73HI 93731-01 100 zinc testsHI 93731-03 300 zinc testsHI 93732-01 100 dissolved oxygen testsHI 93732-03 300 dissolved oxygen testsHI 93737-01 50 silve

74WARRANTYAll Hanna Instruments meters are warranted for two years against defects in workmanship and materialswhen used for its intended purpose and

75HANNA LITERATUREHanna publishes a wide range of catalogs and handbooks for an equally wide range of applications. Thereference literature currently

76Printed in EUROPE(ROMANIA)Hanna Instruments Inc.Highland Industrial Park584 Park East DriveWoonsocket, RI 02895 USATechnical Support for CustomersTe

8The instructions listed below should be carefully followed during testing to ensure most accurate results.• Color or suspended matter in large amount

9• Proper use of the powder reagent packet:(a) use scissors to open the powder packet;(b) push the edges of the packet to form a spout;(c) pour out th