Hanna-instruments HI 83208 Manual do Utilizador Página 1

Consulte online ou descarregue Manual do Utilizador para Instrumentos de medida Hanna-instruments HI 83208. Hanna Instruments HI 83208 User Manual Manual do Utilizador

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Página 1 - HI 83208

1Instruction ManualHI 83208Multiparameter BenchPhotometerfor Water Conditioningwww.hannainst.com

Página 2 - TABLE OF CONTENTS

10• Pay attention to push the cuvette completely down in the holder and to align the white point on thecap to the indexing mark on the meter.• In orde

Página 3 - GENERAL DESCRIPTION

11METHOD REFERENCE TABLEMethod Method Pagedescription1 Ammonia MR 172 Ammonia LR 193 Free Chlorine 214 Total Chlorine 245 Copper HR 276 Copper LR 297

Página 4 - SPECIFICATIONS

12POWER CONNECTION AND BATTERY MANAGEMENTThe meter can be powered from an AC/DC adapter (included) or from the built-in rechargeable battery.Note: Alw

Página 5

13DATA MANAGEMENTThe instrument features a data log function to help you keep track of all your analysis. The data log canhold 200 individual measurem

Página 6 - FUNCTIONAL DESCRIPTION

14In the Setup mode the instrument’s parameters can be changed. Some parameters affect the measuringsequence and others are general parameters that ch

Página 7 - KEYPAD DESCRIPTION

15Date / TimeThis option is used to set the instrument’s date and time.Press the Modify key to change the date/time.Press the W X functional keys to h

Página 8

16HI 83208 offers an interactive contextual help mode that assists the user at any time.To access the help screens press HELP.The instrument will disp

Página 9 - USING CUVETTES

17Ammonia MRSPECIFICATIONSRange 0.00 to 10.00 mg/LResolution 0.01 mg/LAccuracy ±0.05 mg/L ±5% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight

Página 10 - INTERFERENCES

18• Remove the cuvette.• Add 4 drops of HI 93715A-0 First reagent (6 drops forseawater analysis). Replace the cap and mix the solution.• Add 4 drops o

Página 11 - HEALTH & SAFETY

19Ammonia LRSPECIFICATIONSRange 0.00 to 3.00 mg/LResolution 0.01 mg/LAccuracy ±0.04 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight S

Página 12 - OPERATIONAL GUIDE

2Dear Customer,Thank you for choosing a Hanna product. Please read this instruction manual carefully before using theinstrument. This manual will prov

Página 13 - CHEMICAL FORM

20Ammonia LR• Remove the cuvette.• Add 4 drops of HI 93700A-0 First reagent (6 drops forseawater analysis). Replace the cap and mix the solution.• Add

Página 14 - SETUPSETUP

21FREE CHLORINEFREE CHLORINEFREE CHLORINEFREE CHLORINEFREE CHLORINESPECIFICATIONSRange 0.00 to 2.50 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of

Página 15

22Free Chlorine• Press the Zero key. The meter will show “-0.0-” when the meter is zeroed and ready for measurement.• Remove the cuvette.Powder reagen

Página 16 - HELP MODEHELP MODE

23• Reinsert the cuvette into the instrument.• Press Read to start the reading. The instrument displays the results in mg/L of free chlorine.INTERFER

Página 17 - AMMONIA MEDIUM RANGE

24Total ChlorineTOTAL CHLORINESPECIFICATIONSRange 0.00 to 3.50 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±

Página 18

25Total Chlorine• Press the Zero key. The meter will show “-0.0-” when the meter is zeroed and ready for measurement.• Remove the cuvette.Powder reage

Página 19 - AMMONIA LOW RANGE

26• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitfor 2 minutes and 30 seconds and press Read. W

Página 20

27Copper HRCOPPER HIGH RANGESPECIFICATIONSRange 0.00 to 5.00 mg/LResolution 0.01 mg/LAccuracy ±0.02 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/L

Página 21 - FREE CHLORINE

28Copper HR• Remove the cuvette.• Add the content of one packet of HI 93702-0 Bicinchoninate.Replace the cap and shake gently for about 15 seconds.• R

Página 22 - Free Chlorine

29Copper LRCOPPER LOW RANGESPECIFICATIONSRange 0 to 1000 μg/LResolution 1 μg/LAccuracy ±10 μg/L ±5% of reading at 25 °CTypical EMC ±1 μg/LDeviationLig

Página 23

3PRELIMINARY EXAMINATIONPlease examine this product carefully. Make sure that the instrument is not damaged. If any damageoccurred during shipment, pl

Página 24 - TOTAL CHLORINE

30Copper LR• Remove the cuvette.• Add the content of one packet of HI 95747-0 Bicinchoninate.Replace the cap and shake gently for about 15 seconds.• R

Página 25 - Total Chlorine

31FluorideFLUORIDESPECIFICATIONSRange 0.00 to 2.00 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationL

Página 26

32• Press Timer and the display will show the countdown prior to zeroing or, alternatively, wait for twominutes and press Zero. The display will show

Página 27 - COPPER HIGH RANGE

33Iron HRIRON HIGH RANGESPECIFICATIONSRange 0.00 to 5.00 mg/LResolution 0.01 mg/LAccuracy ±0.04 mg/L ±2% of reading at 25 °CTypical EMC ±0.01 mg/LDevi

Página 28

34Iron HR• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternatively,w

Página 29 - COPPER LOW RANGE

35Iron LRIRON LOW RANGESPECIFICATIONSRange 0 to 400 μg/LResolution 1 μg/LAccuracy ±10 μg/L ±8% of reading at 25 °CTypical EMC ±1 μg/LDeviationLight So

Página 30

36Iron LR• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready formeasurement.• Remove the cuvette.• Fill another gra

Página 31 - FLUORIDE

37Iron LRINTERFERENCESInterference may be caused by:Cadmium above 4.0 mg/LChromium3+ above 0.25 mg/LChromium6+ above 1.2 mg/LCobalt above 0.05 mg/LCop

Página 32

38SPECIFICATIONSRange 0.0 to 20.0 mg/LResolution 0.1 mg/LAccuracy ±0.2 mg/L ±3% of reading at 25 °CTypical EMC ±0.1 mg/LDeviationLight Source Tungsten

Página 33 - IRON HIGH RANGE

39Manganese HR• Add the content of one packet of HI 93709B-0 SodiumPeriodate reagent. Replace the cap and invert to mix withgently movements for 2 min

Página 34

4PRINCIPLE OF OPERATIONAbsorption of light is a typical phenomenon of interaction between electromagnetic radiation and matter.When a light beam cross

Página 35 - IRON LOW RANGE

40Manganese LRMANGANESE LOW RANGESPECIFICATIONSRange 0 to 300 μg/LResolution 1 μg/LAccuracy ±10 μg/L ±3% of reading at 25 °CTypical EMC ±1 μg/LDeviati

Página 36

41Manganese LR• Add 0.2 mL of the HI 93748B-0 Alkaline-cyanidereagent solution to each cuvette, replace the caps andinvert gently to mix for about 30

Página 37

42Manganese LR• Insert the second cuvette with the reacted sample intothe instrument.• Press Read to start the reading. The instrument displays the re

Página 38 - MANGANESE HIGH RANGE

43MolybdenumMOLYBDENUMSPECIFICATIONSRange 0.0 to 40.0 mg/LResolution 0.1 mg/LAccuracy ±0.3 mg/L ±5% of reading at 25 °CTypical EMC ±0.1 mg/LDeviationL

Página 39

44• Fill one graduated mixing cylinder up to the 25 mLmark with the sample.• Add the content of one packet of HI 93730A-0molybdenum reagent, close the

Página 40 - MANGANESE LOW RANGE

45Molybdenum• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitfor five minutes and press Read. Whe

Página 41 - Manganese LR

46Nickel HRSPECIFICATIONSRange 0.00 to 7.00 g/LResolution 0.01 g/LAccuracy ±0.07 g/L ±4% of reading at 25 °CTypical EMC ±0.02 g/LDeviationLight Source

Página 42

47Nickel HR• Remove the cuvette and add the content of one packet ofHI 93726-0 reagent. Replace the cap and shake gentlyuntil completely dissolved.• R

Página 43 - MOLYBDENUM

48Nickel LRNICKEL LOW RANGESPECIFICATIONSRange 0.000 to 1.000 mg/LResolution 0.001 mg/LAccuracy ±0.010 mg/L ±7% of reading at 25 °CTypical EMC ±0.001

Página 44 - Molybdenum

49Nickel LR• Press Timer and the display will show a countdown prior to adding reagent C or, alternatively, waitfor 15 minutes. Add one packet of HI 9

Página 45

5Where:-log I/Io= Absorbance (A)Io= intensity of incident light beamI = intensity of light beam after absorptionελ= molar extinction coefficient at wa

Página 46 - NICKEL HIGH RANGE

50INTERFERENCESInterference may be caused by:Co2+ must not be presentFe2+ must not be presentAl3+ above 32 mg/LCa2+ above 1000 mg/L (as CaCO3)Cd2+ abo

Página 47

51NitrateSPECIFICATIONSRange 0.0 to 30.0 mg/LResolution 0.1 mg/LAccuracy ±0.5 mg/L ±10% of reading at 25 °CTypical EMC ±0.1 mg/LDeviationLight Source

Página 48 - NICKEL LOW RANGE

52Nitrate• Replace the cap and immediately shake vigorously upand down for exactly 10 seconds. Continue to mix byinverting the cuvette gently for 50 s

Página 49 - Nickel LR

53Dissolved OxygenSPECIFICATIONSRange 0.0 to 10.0 mg/LResolution 0.1 mg/LAccuracy ±0.4 mg/L ±3% of reading at 25 °CTypical EMC ± 0.1 mg/LDeviationLigh

Página 50

54Dissolved Oxygen• Let the sample stand and the flocculent agent will start to settle.• After approximately 2 minutes, when the upper half of the bot

Página 51 - MEASUREMENT PROCEDURE

55pHpHSPECIFICATIONSRange 6.5 to 8.5 pHResolution 0.1 pHAccuracy ±0.1 pH at 25 °CTypical EMC ±0.1 pHDeviationLight Source Tungsten lamp with narrow ba

Página 52

56pH• Remove the cuvette and add 5 drops of HI 93710-0 PhenolRed Indicator. Replace the cap and mix the solution.• Reinsert the cuvette into the instr

Página 53 - DISSOLVED OXYGEN

57Phosphate HRPHOSPHATE HIGH RANGESPECIFICATIONSRange 0.0 to 30.0 mg/LResolution 0.1 mg/LAccuracy ±1 mg/L ±4% of reading at 25 °CTypical EMC Dev. ±0.1

Página 54

58Phosphate HR• Add the content of one packet of HI 93717B-0 PhosphateHR Reagent B to the cuvette. Replace the cap and shakegently until completely di

Página 55

59Phosphate LRPHOSPHATE LOW RANGESPECIFICATIONSRange 0.00 to 2.50 mg/LResolution 0.01 mg/LAccuracy ±0.04 mg/L ±4% of reading at 25 °CTypical EMC Dev.

Página 56

6INSTRUMENT DESCRIPTION1) Open Cuvette Lid2) Indexing mark3) Cuvette point4) Liquid Crystal Display (LCD)5) Splash proof keypad6) ON/OFF power switch7

Página 57 - PHOSPHATE HIGH RANGE

60Phosphate LR• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternativ

Página 58

61PhosphorusPHOSPHORUSSPECIFICATIONSRange 0.0 to 15.0 mg/LResolution 0.1 mg/LAccuracy ±0.3 mg/L ±4% of reading at 25 °CTypical EMC Dev. ±0.2 mg/LLight

Página 59 - PHOSPHATE LOW RANGE

62Phosphorus• Add the content of one packet of HI 93706B-0 PhosphorusReagent B (Amino Acid) to the cuvette. Replace the capand shake gently until comp

Página 60

63SilicaSILICASPECIFICATIONSRange 0.00 to 2.00 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight

Página 61 - PHOSPHORUS

64Silica• Place the cuvette into the holder and close the lid.• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready f

Página 62

65• Press  or  to return to the measurement screen.INTERFERENCESInterference may be caused by:Phosphate above 60 mg/LPhosphate above 75 mg/LSulfide

Página 63

66SilverSILVERSPECIFICATIONSRange 0.000 to 1.000 mg/LResolution 0.005 mg/LAccuracy ±0.020 mg/L ±5% of reading at 25 °CTypical EMC ± 0.001 mg/LDeviatio

Página 64

67Silver• Add exactly 1.0 mL of HI 93737B-0 Buffer reagent to the secondbeaker (the sample) and swirl gently to mix. Press Timer and thedisplay will s

Página 65

68Silver• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready formeasurement.• Fill a second cuvette up to the mark w

Página 66

69ZincZINCSPECIFICATIONSRange 0.00 to 3.00 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight Sou

Página 67

7KEYPAD DESCRIPTIONThe keypad contains 8 direct keys and 3 functional keys with the following functions:Press to perform the function displayed above

Página 68

70INTERFERENCESInterference may be caused by:Aluminum above 6 mg/LCadmium above 0.5 mg/LCopper above 5 mg/LIron above 7 mg/LManganese above 5 mg/LNick

Página 69 - REQUIRED REAGENT

71The instrument shows clear warning messages when erroneous conditions appear and when measured values areoutside the expected range. These messages

Página 70

72Description Range MethodAmmonia MR 0.00 to 10.00 mg/ L NesslerAmmonia LR 0.00 to 3.00 mg /L NesslerChlorine, Free 0.00 to 2.50 mg/L DPDChlorine, Tot

Página 71 - ERRORS AND WARNINGS

73Nickel LR 0.000 to 1.000 mg/L PANNitrate 0.0 to 30.0 mg/ L Cadmium ReductionOxygen, Dissolved 0.0 to 10.0 mg/L WinklerpH 6.5 to 8.5 pH Phenol RedPho

Página 72 - STANDARD METHODS

74HI 93726-01 100 nickel HR testsHI 93726-03 300 nickel HR testsHI 93728-01 100 nitrate testsHI 93728-03 300 nitrate testsHI 93729-01 100 fluoride tes

Página 73 - ACCESSORIES

75WARRANTYAll Hanna Instruments meters are warranted for two years against defects in workmanship and materialswhen used for its intended purpose and

Página 74

76Printed in EUROPE(ROMANIA)Hanna Instruments Inc.Highland Industrial Park584 Park East DriveWoonsocket, RI 02895 USATechnical Support for CustomersTe

Página 75 - HANNA LITERATURE

8The instructions listed below should be carefully followed during testing to ensure most accurate results.• Color or suspended matter in large amount

Página 76 - MAN83208 04/10

9• Proper use of the powder reagent packet:(a) use scissors to open the powder packet;(b) push the edges of the packet to form a spout;(c) pour out th

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